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語文別: 英文. 論文頁數: 183. 論文摘要本論文係探討新型氣旋式大氣電漿改質技術應用於多孔性膜與相關材料之表面特性分析。

為利用氣旋式大氣電漿改質氧化銦錫薄膜、聚 ... 資料載入處理中... 跳到主要內容 臺灣博碩士論文加值系統 ::: 網站導覽| 首頁| 關於本站| 聯絡我們| 國圖首頁| 常見問題| 操作說明 English |FB專頁 |Mobile 免費會員 登入| 註冊 功能切換導覽列 (165.22.59.181)您好！臺灣時間：2021/11/2506:56 字體大小：       ::: 詳目顯示 recordfocus 第1筆/ 共1筆  /1頁 論文基本資料 摘要 外文摘要 目次 參考文獻 紙本論文 論文連結 QRCode 本論文永久網址: 複製永久網址Twitter研究生:蔡景元研究生(外文):Ching-YuanTsai論文名稱:以氣旋式大氣電漿進行多孔性膜與相關材料之表面改質研究論文名稱(外文):InvestigationofCyclonicAtmosphericPressurePlasmaModificationProcessonPlasmaModifiedPorousMembraneandRelatedMaterialSurfaceCharacterization指導教授:黃駿、莊瑞鑫指導教授(外文):ChunHuang、Ruey-ShinJuang口試委員:魏大欽、陳克紹、何政恩、劉志宏口試委員(外文):Ta-ChinWei、Ko-ShaoChen、Cheng-EnHo、Chih-HungLiu口試日期:2013-06-24學位類別:博士校院名稱:元智大學系所名稱:化學工程與材料科學學系學門:工程學門學類:化學工程學類論文種類:學術論文論文出版年:2013畢業學年度:101語文別:英文論文頁數:183中文關鍵詞:氣旋式大氣電漿、表面改質、多孔性膜、親水性外文關鍵詞:cyclonicatmospheric-pressureplasma、surfacemodification、porousmembrane、hydrophilicity相關次數: 被引用:1點閱:267評分:下載:0書目收藏:0 本論文係探討新型氣旋式大氣電漿改質技術應用於多孔性膜與相關材料之表面特性分析。

為利用氣旋式大氣電漿改質氧化銦錫薄膜、聚碸薄膜、聚丙烯不織布以及316不銹鋼，並且包含通入六甲基二矽氧烷(HMDSO)沉積矽氧膜於聚偏二氟乙烯(PVDF)薄膜以改善其親水性。

實驗過程中，藉由改變電漿功率、改質時間、氣體流率以及基材至噴頭距離等電漿條件，探討親疏水特性、表面自由能、表面型態、表面粗糙度、表面元素及細胞貼附性之變化。

親疏水特性分析則以靜態接觸角量測儀進行分析，可知其多孔性膜與相關材料表面經由氣旋式大氣電漿改質過後，材料因電漿中CASING效應使得表面呈現超親水現象，另沉積矽氧膜於聚偏二氟乙烯膜表面亦呈現親水特性。

實驗結果之物理特性分析方面，使用場發射掃描式電子顯微鏡以及原子力顯微鏡進行表面型態、表面粗糙度變化之分析研究。

至於化學性質分析方面，則使用X射線光電子能譜儀探討表面元素與鍵結之變化。

於實驗過程中搭配光放射光譜儀觀察氣旋式大氣電漿內物種特性分析以進行表面變化之佐證。

最後於靜態接觸角結果方面得知，氧化銦錫薄膜、聚碸薄膜、聚丙烯不織布以及316不銹鋼分別最低可達到8°、8°、0°以及3°。

並可知利用氣旋式大氣電漿改質相關材料之水滴接觸角變化呈現出高分子多孔性薄膜、半導體以及導體三大區域。

另一方面利用前驅物六甲基二矽氧烷沉積矽氧膜於聚偏二氟乙烯膜上，水滴接觸角明顯地從137°降低至38°。

從本論文研究可知，利用氣旋式大氣電漿改質技術可有效的改善相關材料表面親水特性並且提升其材料表面自由能，而對於導體材料最易改善其親水性之效果。

並由接觸角所呈現之三區域得知，往後利用氣旋式大氣電漿改質不同材料所需之改質能量其多寡，以利於不同材料表面改質之應用。

Inthisinvestigation,cyclonicatmospheric-pressureplasmaprocessingwasconductedtostudytheplasma-modifiedporousmembraneandrelatedmaterialsurfacemodificationeffect,includingITOfilm,polysulfonemembrane,non-wovenpolypropyleneand316stainlesssteel.Inaddition,alsousingcyclonicatmospheric-pressureplasma-depositedorganosiliconfilmonpolyvinylidenefluoride(PVDF)membranefromargon/hexamethyldisoxane(HMDSO)mixtures.Thechangeofhydrophilicitywasmonitoredbystaticcontactanglemeasurement.Thematerialsurfacebecamehighlyhydrophilicwhenexposedtothecyclonicatmospheric-pressureplasma.Thesurfacemodificationeffectsofplasmaoperationalconditionsincludingtreatmenttime,plasmapower,gasflowrate,anddistanceofnozzletosubstrateonthematerialsurfacefeatureswereexamined.AsignificantincreaseinthesurfacefreeenergyofmaterialsurfaceduetoCASINGeffectandorganosiliconfilmwasobserved.Opticalemissionspectroscopy(OES)wasemployedtoinvestigatethevariouschemicalspeciesofcyclonicatmospheric-pressureplasmaprocessing.ChemicalstructureandsurfacemorphologicalchangesonthematerialsurfacewerecharacterizedbyX-rayphotoelectronspectroscopy(XPS),fieldemissionscanningelectronmicroscopy(FE-SEM)andatomicforcemicroscopy(AFM).XPSanalysisshowedsignificantlyhighersurfaceconcentrationsofoxygenfunctionalgroupsforcyclonicatmospheric-pressureplasma-activatedmaterialsurfacethanoriginallyunmodifiedmaterialsurface.MG-63cell-adhesiononthenon-wovenpolypropyleneand316stainlesssteelsurfacewerecharacterizedbyfluorescencemicroscope.ThestaticcontactangleofDIwateronthecyclonicatmospheric-pressureplasma-modifiedITOfilm,polysulfonemembrane,non-wovenpolypropyleneand316stainlesssteeldecreasedsignificantlyto8°、8°、0°and3°,respectively.Aboutcontactangledataofrelatedmaterialcanbedividedintothreeregions,includingtheporouspolymericmembrane,semiconductor,andconductor.Thestaticcontactangleofcyclonicatmospheric-pressureplasma-depositedorganosiliconfilmonPVDFmembranedecreasedsignificantlyfrom137°to38°.Theexperimentalresultsrevealthatcyclonicatmospheric-pressureplasmaprocessingisaneffectivemethodtoimprovethesurfacehydrophilicityofmaterialsurface,andeasytomodifytheconductormaterial. 摘要IABSTRACTIIIACKNOWLEDGEMENT/誌謝VCONTENTSVIILISTOFFIGURESXILISTOFTABLESXXIVCHAPTER1INTRODUCTION11.1Atmospheric-pressureplasma11.2Purposeofresearch3CHAPTER2LITERATUREREVIEW52.1Plasma52.2Equilibriumandnon-equilibriumdischargeplasma62.3Thedifferentkindsofatmospheric-pressureplasma92.4Plasmamodification122.5Comparisonofotheratmospheric-pressureplasmasurfacemodificationsystem142.6Recentdevelopmentofcyclonicatmospheric-pressureplasmasystem17CHAPTER3EXPERIMENTALDETAILS203.1.Cyclonicatmospheric-pressureplasmasystem203.1.1TemperatureprofileonvariousRFplasmapower233.1.2OpticalemissionspectroscopyanalysiswithvariousRFplasmapower263.1.3ElectricalCharacterizationwithvariousplasmaparameters273.2.Modifiedsurfacecharacterizationandanalysis333.2.1MaterialsandPre-treatment333.2.2StaticcontactangleandSurfacefreeenergy343.2.3OpticalEmissionSpectroscopy383.2.4Atomicforcemicroscopy393.2.5Scanningelectronmicroscopy&Fieldemissionscanningelectronmicroscopy403.2.6X-rayphotoelectronspectroscopy413.2.7SurfaceAreaandPorosityAnalyzerorosimetry423.2.8MeasurementFilmSystem433.2.9MeasurementInstrumentsofElectricalCharacterization443.2.10CellcultureandCellmorphology(Fluorescencestaining)453.2.11Filtersystem47CHAPTER4RESULTSANDDISCUSSION484.1Cyclonicatmospheric-pressureplasmamodificationonvariousmaterialsurface484.1.1SurfacetreatmentandcharacterizationofITOthinfilmsusingcyclonicatmosphericpressureplasma484.1.2Surfacehydrophilizationofpolysulfonemembranebycyclonicatmosphericpressureplasma644.1.3Surfacetreatmentofnon-wovenpolypropylenebycyclonicatmosphericpressureplasma834.1.4Surfacetreatmentof316stainlesssteelbycyclonicatmosphericpressureplasma974.1.5Opticalemissionspectroscopyanalysis1124.1.6Plasmatreatmentonvariousmaterialsurfaceofcyclonicatmosphericpressureplasmasystem1194.2Preparingpolyvinylidenefluoride(PVDF)compositemembranebycyclonicatmospheric-pressureplasmadepositedorganosiliconfilm1224.2.1Cyclonicatmospheric-pressureplasmadepositedorganosiliconfilm1224.2.2XPSanalyzeorganosiliconfilmonPVDFmemnrane1364.2.3SEManalyzeorganosiliconfilmonPVDFmemnrane1454.2.4Membranepermeabilitytest147CHAPTER5CONCLUSION149REFERENCES152LISTOFPUBLICATION174Journalpaper174Conferencepaper177Award183 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 國圖紙本論文 連結至畢業學校之論文網頁點我開啟連結註:此連結為研究生畢業學校所提供，不一定有電子全文可供下載，若連結有誤，請點選上方之〝勘誤回報〞功能，我們會盡快修正，謝謝！ 推文 網路書籤 推薦 評分 引用網址 轉寄                                                                                                                                                                                                                    top 相關論文 相關期刊 熱門點閱論文 1. 利用十三氟辛基三乙氧基矽烷進行噴射式大氣電漿束沉積疏水薄膜之研究 2. 石墨包裹奈米鐵晶粒的純化及表面改質程序之研究 3. 利用氮氣為主的常壓電漿束於聚乳酸材料表面快速植入胺基官能基之研究 4. 多巴胺披覆金奈米粒子於高效能濕度感測器之應用 5. 溶液聚合法製備水性壓克力樹脂塗佈於PET薄膜之研究 6. 水性聚氨酯改質PET薄膜之表面性質研究 7. 利用聚乙烯吡咯烷酮表面改質對矽水膠隱形眼鏡潤濕性之探討 8. 大氣電漿應用於工業級和生醫級聚醚醚酮表面親水性改質之研究 9. 生物燃料電池石墨氈陽極材料改質與特性分析 10. 表面處理對基材/OCA界面相互作用力影響效應之研究 11. 液滴在具結構表面的濕潤行為與親疏水表面接觸角定量定義探討 12. 探討矽氧烷基親水性高分子改質矽膠表面降低非特異性蛋白質吸附 13. 利用電容耦合式管型電漿對單層聚乙烯膜進行活化處理及其表面性質分析 14. 豬籠草唇之啟發:以生物翻模與表面處理技術合成多功能表面之微結構分析與濕潤性質量測 15. 以鎳反蛋白石結構進行親水與疏水之表面改質研究   無相關期刊   1. 以低壓電漿表面改質技術應用於醋酸纖維薄膜與聚丙烯薄膜表面研究 2. 利用氣旋式大氣電漿對緻密型聚苯乙烯進行活化與接枝丙烯酸研究 3. 利用六甲基二矽氮烷與六甲基二矽氧烷大氣電漿聚合超疏水奈米薄膜研究 4. 以大氣電漿束蝕刻矽晶片及光阻膜之研究 5. 大氣電漿束之電漿特性與應用之研究 6. 以大氣電漿及矽烷化處理於羽毛表面合成多功能超疏水及疏油塗層 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